WSU Chemistry 410
This channel provides videos of chemical experiments and laboratory techniques undertaken in Chemistry 410: Advanced Synthesis and Characterization at Washington State University
Experiment 12, Synthesis of Me5CpIrCl2 Dimer
Using a McLeod Gauge to Measure Vacuum Pressure
Using Rubberbands in Schlenk Line Manipulations
Removing Solvent on a Schlenk Line
Experiment #11 Synthesis of KBArF4, Cp2FeBArF4, and AgBArF4
Experiment #6, Synthesis of 8-SMe-BODIPY
Vacuum Distillation
Air/Moisture Sensitive Filtrations
Preparation of an NMR Sample
Experiment #1, Glow Sticks
COVID-19 Disinfection Procedure
Experiment #2, Silicone Polymers
Experiment #7, Thermochromic Compounds
Experiment #3, Synthesis of Mn(acac)3
Operation of 500 MHz Varian NMR Spectrometer
Experiment #8, Synthesis and Decomposition of tBuNH2BH3
Greasing and Degreasing Ground Glass Joints
Experiment #4, Synthesis of (η6-Mesitylene)Mo(CO)3
Using a Rotary Evaporator
Experiment #9, Sublimation of Ferrocene and Synthesis of Cp2FePF6
Cooling Chemical Reactions
Heating Chemical Reactions
Collecting Liquid Nitrogen from a Dewar/Lockset
Experiment #5, Synthesis and Reactivity of Vaska's Complex
Setting Up & Taking Down a Schlenk Line
Transferring Solvents & Reagents with a Syringe on a Schlenk Line
Transferring Solvents & Reagents with a Cannula on a Schlenk Line
Introduction to Schlenk Lines
Using the Glovebox Antechambers/Ports
Introduction to a Glovebox